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Instrumentation LC-MS/MS analyses were carried out with a Thermo Accela UPLC pump and Pal Autosampler interfaced to a Thermo Vantage triple-stage quadrupole mass spectrometer, or with a Thermo/Dionex UltiMate 3000 RS Pump UPLC+ Focused UPLC and CTC/Dionex UltiMate 3000 XRS Open Autosampler interfaced to a Thermo Quantiva triple-stage quadruple mass spectrometer

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