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Higher-order structure characterisation through techniques such as NMR, circular dichroism (CD), and FTIR Stability studies to assess degradation pathways including oxidation, deamidation, and oligomerisation Importantly, formulation components can interfere with detection (e.g., UV-active excipients), requiring careful method design and sample preparation strategies such as buffer exchange

This level of care and attention to detail is what separates a successful experiment from an unsuccessful one

Supplementary Materials Acknowledgements DP is guarantor for CAMERA data and ERP for DIRECT data

Batch-linked CoAs are issued on request to verified laboratory accounts